
New TopShim run:

version = topshim 2.0.0
date = 2024-09-18
time = 00:03:30.664
command = topshim 

FINE SHIMMING

Parameters:

probe = Z168772_0022
solvent = CDCl3
shim nucleus = 2H
nucleus optimised for = 1H
o1p (from lock) = 7.24 ppm

Results:


1D Shimming:
Iteration  1: FWHM Before= 1.2 Hz, Target= 0.2 Hz, After= 2.7 Hz
Iteration  2: FWHM Before= 2.7 Hz, Target= 0.2 Hz, After= 1.8 Hz
Iteration  3: FWHM Before= 1.8 Hz, Target= 0.7 Hz, After= 1.4 Hz
Iteration  4: FWHM Before= 1.4 Hz, Target= 0.4 Hz, After= 0.5 Hz
Iteration  5: FWHM Before= 0.5 Hz, Target= 0.4 Hz, After= 0.7 Hz
Iteration  6: FWHM Before= 0.7 Hz, Target= 0.5 Hz
Shim succeeded

Lineshape quality factor (1D spectrum, spinning) = 1.31

shim changes: 
Z	-723
Z2	-286
Z3	-588
Z4	-2604
Z5	-1524

duration = 4 min 0 sec
completed successfully
finished Wed Sep 18 00:07:29 2024


========================================================================

New TopShim run:

version = topshim 2.0.0
date = 2024-09-18
time = 00:07:41.383
command = topshim  tunea tune

TUNE

Parameters:

probe = Z168772_0022
solvent = CDCl3

Results:


Performing tune after shimming
tune lock level increase = 1.0

shim changes: 
Z	-7
X	+20
XZ	+27
Y	+27
YZ	+29

duration = 1 min 11 sec
completed successfully
finished Wed Sep 18 00:08:51 2024


========================================================================

New TopShim run:

version = topshim 2.0.0
date = 2024-09-18
time = 00:09:14.443
command = topshim 

FINE SHIMMING

Parameters:

probe = Z168772_0022
solvent = CDCl3
shim nucleus = 2H
nucleus optimised for = 1H
o1p (from lock) = 7.24 ppm

Results:


1D Shimming:
Iteration  1: FWHM Before= 0.5 Hz, Target= 0.2 Hz, After= 1.6 Hz
Iteration  2: FWHM Before= 1.6 Hz, Target= 0.5 Hz, After= 0.8 Hz
Iteration  3: FWHM Before= 0.8 Hz, Target= 0.3 Hz, After= 1.5 Hz
Iteration  4: FWHM Before= 1.5 Hz, Target= 0.4 Hz, After= 0.5 Hz
Iteration  5: FWHM Before= 0.5 Hz, Target= 0.4 Hz, After= 1.0 Hz
Iteration  6: FWHM Before= 1.0 Hz, Target= 0.4 Hz, After= 0.9 Hz
Rejecting all results and reverting to the initial shim state.

Lineshape quality factor (1D spectrum, spinning) = 1.15

shim changes: none

duration = 3 min 46 sec
completed successfully
finished Wed Sep 18 00:12:59 2024


========================================================================
